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Chemistry, 22.06.2019 08:00
Straightforward questions answered in the powerpoint slidesreaction: heating the starting materials under refluxwhat does it mean to heat under reflux? why do we choose water as the reflux solvent? what are boiling chips used for? why do we put a condenser on top of the reaction? why do we add heat and let the reaction stir for 30 minutes? why do we add sulfuric acid to the reaction after it cools as opposed to when it’s still hot? separation: filtration of precipitatewhy don’t we do an aqueous and organic extraction in the separatory funnel? why do you rinse the salicylic acid on the filter with ice cold water? purification: recrystallization of salicylic acid (no hot filtration needed)what is the difference in the amount of room temperature water vs. boiling water needed to dissolve the salicylic acid (assume a 1.2 gram yield of salicylic acid)? remember, in the lab if you need x ml of boiling water to dissolve a solid, then you should add a little more (definitely no more than 1.5 times the theoretical amount) to ensure it doesn’t recrystallize prematurely.analysis: melting point of salicylic acidwhat can you conclude if the melting point of the salicylic acid you just synthesized is 152-155oc and the 1: 1 mix of your product and “synthetic” salicylic acid is 151-154oc?
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Chemistry, 22.06.2019 12:40
Quiz1. which physical state of nitrogen has the highest entropy? a solid© b gasoc liquid
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Chemistry, 23.06.2019 03:00
Achemical equilibrium between gaseous reactants and products is shown. n2(g) + 3h2(g) ⇌ 2nh3(g) how will the reaction be affected if the pressure on the system is increased? it will shift toward the reactant side as there is lower pressure on the reactant side. it will shift toward the product side as there is higher pressure on the product side. it will shift toward the reactant side as there are a greater number of moles of gas on the reactant side. it will shift toward the product side as there are a fewer number of moles of gas on the product side.
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